Epoxy resin was analyzed using GPC HK-402, an organic SEC (GPC) column for ultra-rapid analysis, and GPC KF-802.5 which is a conventional type column supports similar target molecular weight range for HK-402. When using HK-402 at the same flow rate as the conventinal type column, the same separation can be obtained in less than 1/6 of the analysis time. The HK-400 series has a low column pressure even at high flow rates and can be used in conventional HPLC device.
Sample :
jER1001 (Epoxy resin) 0.2 %(w/v)
10 µL (HK-402)
50 µL (KF-802.5)
Columns : Shodex GPC HK-402 (4.6 mm I.D. x 150 mm) Shodex GPC KF-802.5 (8.0 mm I.D. x 300 mm) Eluent : THF Flow rate : 1.0 mL/min Detector : UV (254 nm) (small cell volume) Column temp. : 40 °C
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