糖的洗脱体积

七种不同色谱柱SUGAR SP0810, SC1011, KS-801, SZ5532, SC1211, RSpak DC-613, Asahipak NH2P-50 4E和GS-220 HQ 对糖的洗脱体积见下表。
表中只提供了出峰的位置，如果希望看到实际的色谱峰宽，请和我们联系。

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Substances	Elution Volume (mL)
	SUGAR					RSpak	Asahipak
	SP0810	SC1011	KS-801	SZ5532	SC1211	DC-613	NH2P-50 4E	GS-220 HQ x 2
	Pb²⁺	Ca²⁺	Na⁺	Zn²⁺	Ca²⁺	Na⁺	NH2P-50 4E	GS-220 HQ x 2
N-Acetyl-α-D-glucosamine	8.86	7.75	6.68	2peaks	4.10	2peaks	6.66
D(+)-Arabinose	10.42	8.91	8.21	5.11	5.56	5.75	6.18
D-Arabitol	15.86	11.33	7.63	7.27	8.16	5.81	6.29
Aspartame	-	-	-	-	34.02	-	-
2-Deoxy-D-glucose	8.83	7.58	7.15	4.34	4.02	4.43	6.02
Difructose anhydride III	7.07	6.30	5.81	4.30	*	4.51	7.77
Dulcitol	20.18	12.76	7.40	9.46	11.28	7.33	7.45
meso-Erythritol	12.70	10.09	7.86	5.73	6.27	4.84	5.43	17.38
Ethanol	11.13	11.33	10.09	-	4.27	-	-
1-Fructofuranosyl-D-nystose	6.05	5.27	4.76	31.43	*	-	-	14.24
D(-)-Fructose	11.05	8.85	7.71	5.37	5.90	6.19	6.75	17.05
D(+)-Fucose	10.48	8.84	8.09	4.50	4.96	4.81	5.43
D(+)-Galactose	9.74	7.98	7.58	6.46	4.98	7.28	8.10	16.60
4'-Galactosyllactose	7.42	6.02	5.40	19.02	*	21.24	21.66
α-D-Galacturonic acid	-	6.28	4.36	-	5.63	-	-
Gentiobiose	7.22	6.08	5.75	10.50	*	13.18	16.36
Glucose	8.63	7.30	7.17	5.87	4.76	6.83	8.61	16.75
Glycerol						4.26		17.83
Glycyrrhizin	-	-	-	-	2.71	2.00	-
myo-Inositol	12.77	8.86	7.99	12.63	7.87	15.80	9.96
Isomaltose	7.68	6.26	5.95	10.57	*	13.82	15.18	15.57
Isomaltotriose	7.09	5.75	5.34	21.17	*	32.02	27.55	14.72
1-Kestose	6.79	5.75	5.26	13.09	*	-	20.11	15.31
Kojibiose	7.56	6.21	5.88	9.65	*	11.47	14.82
Lactitol	13.27	8.09	6.13	16.35	6.67	14.04	11.82	15.50
Lactose	8.05	6.51	5.99	10.12	4.07	11.69	13.27	15.71
Lactosyl fructoside	7.12	5.88	5.29	14.69	*	15.75	18.98
Lactulose	9.13	6.99	6.19	9.16	4.65	10.80	10.72
Maltitol	12.23	8.26	6.03	13.04	6.77	11.81	11.82	15.82
Maltoheptaose						-		14.82
Maltohexaose						-		14.56
Maltopentaose						-		14.31
Maltose	7.85	6.34	5.94	8.67	*	10.61	14.24	16.11
Maltotriose	7.48	5.89	5.38	13.79	*	17.88	24.96	15.56
Mannitol	15.80	11.10	7.23	8.75	9.03	6.84	7.39
D-Mannose	10.72	8.17	7.64	5.83	5.01	6.72	7.84
D(+)-Melezitose	6.94	5.79	5.24	13.60	*	14.68	19.27
Melibiose	8.16	6.45	5.98	11.69	4.23	14.83	14.70
Methyl-α-D-mannopyranoside	11.13	8.87	7.78	3.99	4.39	4.15	4.71
Nystose	6.38	5.45	4.93	20.05	*	-	31.90	14.72
Palatinit	2peaks	2peaks	5.90	2peaks	2peaks	2peaks	12.73
Palatinose	7.84	6.45	5.89	8.08	3.99	9.81	12.12
Panose	7.14	5.78	5.32	16.87	*	23.14	25.60
L-Phenylalanine	-	-	-	-	31.58	-	-
D(+)-Raffinose	7.14	5.78	5.29	16.36	*	19.11	20.25	15.08
D(+)-Rhamnose	9.77	8.23	7.37	3.93	4.43	4.09	5.52
D(-)-Ribose	19.35	13.66	9.04	4.82	8.64	5.30	5.45
Rutinose	7.81	6.49	5.80	6.65	*	7.21	10.87
Saccharin sodium	6.96	5.44	4.33	6.77	*	2.04	5.68
D(-)-Sorbitol	21.61	13.31	7.42	9.79	11.88	7.27	7.09	16.60
D(+)-Sorbose	9.67	8.03	7.38	5.12	4.92	5.91	7.35
Stachyose	6.82	5.57	4.97	-	*	-	36.22	14.33
Stevioside	-	-	-	4.14	*	4.44	6.07
Sucrose	7.54	6.29	5.87	7.91	*	8.68	11.87	16.26
α-D-Talose	21.33	12.59	8.76	5.69	8.51	6.32	6.47
Theanderose	2peaks	2peaks	2peaks	2peaks	*		2peaks
Trehalose	7.62	6.27	5.78	10.85	*	11.49	13.25
Trehalulose	8.92	6.95	6.10	9.54	4.78	11.38	11.68
Xylitol	19.87	13.14	7.94	7.77	10.16	6.19	6.10	16.88
Xylobiose	8.16	6.68	6.40	5.65	*	6.71	9.05
D(+)-Xylose	9.21	7.90	7.71	4.55	4.48	5.21	6.58	17.46
D-Xylulose	10.64	9.02	8.04	4.06	5.07	4.56	5.41

(-) -> 未检出 (*) -> 与溶剂峰重叠

Columns: ：Shodex SUGAR SP0810, SC1011, KS-801 (8.0 mm I.D. x 300 mm each)
Eluent: ：H₂O
Flow rate: ：1.0 mL/min
Detector: ：RI
Column temp.: ：80 ℃
Column: ：Shodex SUGAR SZ5532 (6.0 mm I.D. x 150 mm)
Eluent: ：H₂O/CH₃CN=25/75
Flow rate: ：1.0 mL/min
Detector: ：RI
Column temp.: ：60 ℃
Column: ：Shodex SUGAR SC1211 (6.0 mm I.D. x 250 mm)
Eluent: ：H₂O/CH₃CN=65/35
Flow rate: ：1.0 mL/minv
Detector: ：RI
Column temp.: ：70 ℃
Column: ：Shodex RSpak DC-613 (6.0 mm I.D. x 150 mm)
Eluent: ：H₂O/CH₃CN=25/75
Flow rate: ：1.0 mL/min
Detector: ：RI
Column temp.: ：70 ℃
Column: ：Shodex Asahipak NH2P-50 4E (4.6 mm I.D. x 250 mm)
Eluent: ：H₂O/CH₃CN=25/75
Flow rate: ：1.0 mL/min
Detector: ：RI
Column temp.: ：30 ℃
Columns: ：Shodex Asahipak GS-220 HQ (7.5 mm I.D. x 300 mm) x 2
Eluent: ：H₂O
Flow rate: ：0.5 mL/min
Detector: ：RI
Column temp.: ：60 ℃

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