样品预处理后使用Silica C18M 4E色谱柱分析黄曲霉毒素。
Sample: 20 μL
5μg/L each
可滚动
| No. | TFA method | PR method |
|---|---|---|
| 1 | Derived Aflatoxin G1 | Aflatoxin G2 |
| 2 | Derived Aflatoxin B1 | Aflatoxin G1 |
| 3 | Aflatoxin G2 | Aflatoxin B2 |
| 4 | Aflatoxin B2 | Aflatoxin B1 |
For TFA method
- Column
- ：Shodex Silica C18M 4E 4.6 mm I.D. x 250 mm)
- Eluent
- ：CH3CN/CH3OH/H2O=10/30/60
- Flow rate
- ：1.0 mL/min
- Detector
- ：Fluorescence (Ex.365 nm, Em.450 nm)
- Column temp.
- ：40 ℃
For PR method
- Column
- ：Shodex Silica C18M 4E (4.6 mm I.D. x 250 mm)
- Eluent
- ：CH3OH/H2O=40/60
- Flow rate
- ：0.7 mL/min
- Detector
- ：Fluorescence (Ex.365 nm, Em.450 nm)
- Column temp.
- ：40 ℃