Please use this column with suppressor type ion chromatography system.
The concentration of sulfur dioxide or sulfite in a pair of disposable wooden chopsticks was decided ≥4 mg(sulfur dioxide equivalent) in Shoku-An No.1113001 (November 13, 2007) of Department of Food Safety, Pharmaceutical and Food Safety Bureau, MHLW. After preparing disposable wooden chopsticks according to the offial method, sulfite was analyzed using a column for anions analysis, IC SI-35 4D.
Preparation of Sample
Pour 25 mL of water into the stoppered test tube (25 mL) and warm it to 95 °C.
Cut one disposable wooden chopstick into two pieces, soak the peices in heated water (95 °C) for 30 minutes, and then remove from the solution.
After the solution cooled downm, dilute 5 mL of the cooled solution with 20 mL of water and filter using a 0.45 μm membrane filter before injection.
Sample : 50 μL
1. SO32-
Column : Shodex IC SI-35 4D (4.0 mm I.D. x 150 mm) Eluent : 3.2 mM Na2CO3 + 1.9 mM NaHCO3 aq. Flow rate : 0.6 mL/min Detector : Suppressed conductivity Column temp. : 40 °C
Sample Name Index
Operation Manual / Certificate of Analysis
Operation Manuals and Certificate of Analysis / Inspection Certificate for the following products can be downloaded here.
Product Name Index
Applications
- Table of Anion Retention Time under Various Eluent Conditions (SI-90 4E)
- Effects of Sodium Carbonate Concentration on Retention Time (SI-90 4E)
- Effects of Sodium Bicarbonate Concentration on Retention Time (SI-90 4E)
- Effects of Temperature on Elution Time (SI-90 4E)
- Effects of Added Acetonitrile on the Retention Time (SI-90 4E)
- Effects of Column Temperature on Retention Time (SI-50 4E)
- Effects of Sodium Carbonate Concentration on Retention Time (SI-50 4E)
- Anion Standards (19) Rapid Analysis (SI-90 4E)
- Anion Standards (20) (Simultaneous Analysis of HS-, SO32-, SO42- and S2O32-) (SI-90 4E)
- Anion Standards (21) (Methanesulfonic Acid)
- High Sensitive Analysis of Anions (SI-90 4E)
- Anion Standards and Organic Acids (2) (SI-90 4E)
- Anion Standards and Organic Acids (3) (SI-50 4E)
- Mineral Water (2) (SI-90 4E)
- Sulfite in Wine (2) (SI-90 4E)
- Sodium Azide (2) (SI-90 4E)
- Sulfamic Acid (SI-90 4E)
- Sea Water (3) (SI-90 4E)
- Perchloric Acid (SI-90 4E)
- Analysis of Iodide Ion (SI-90 4E)
- Fluoroacetid Acids (SI-50 4E)
- Anion Analysis in Lithium Salts (3) (SI-90 4E)
- Analysis of Oxyhalides (SI-52 4E)
- Effects of Temperature on Retention Time (SI-52 4E)
- Calibration Curves for Oxyhalides (SI-52 4E)
- Analysis of Organic Acids and Oxyhalides (SI-52 4E)
- Analysis of Oxyhalides and Anions (SI-52 4E)
- Analysis of Oxyhalides and Anions in River Water (SI-52 4E)
- Analysis of Oxyhalides and Anions in Rain Water (SI-52 4E)
- Analysis of Oxyhalides and Anions in Tap Water (SI-52 4E)
- Iodic Acid (SI-52 4E)
- Separation of Phosphate, Phosphtite and Hypophosphite (SI-52 4E)
- Separation of Phosphate, Phosphtite and Hypophosphite (SI-90 4E)
- Analysis of Chloride According to Japanese Testing Methods for Fertilizers (SI-52 4E)
- Analysis of Sulfate According to Japanese Testing Methods for Fertilizers (SI-90 4E)
- Rapid Analysis of Oxyhalides and Anions (SI-35 4D) (1)
- Rapid Analysis of Oxyhalides and Anions (SI-35 4D) (2)
- Effects of Temperature on Retention Time (SI-35 4D)
- Analysis of Oxyhalides and Anions in Tap Water (SI-35 4D)
- Analysis of Organic Acids and Oxyhalides (SI-35 4D)
- Methanesulfonic Acid and Methanedisulfonic Acid (SI-35 4D)
- Calibration Curves (SI-35 4D)
- Effects of Injection Volume (SI-35 4D)
- Effects of Sample Concentration on Theoretical Plate Number (SI-35 4D)
- Analysis of Tricarboxylic Acids (SI-35 4D)
- Effects of Sodium Carbonate Concentration on Retention Time (SI-35 4D)
- Analysis of Alkyl Sulfonic Acids (2) (SI-35 4D)
- Rapid Analysis of Anion Standards (SI-35 2B)
- Calibration Curves (SI-35 2B)
- Effects of Temperature on Retention Time (SI-35 2B)
- Analysis of Anions (SI-36 4D)
- Effects of Potassium Hydroxide Concentration on Retention Time (SI-36 4D)
- Effects of Potassium Hydroxide Concentration on Retention Time (2) (SI-36 4D)
- Effects of Temperature on Retention Time (SI-36 4D)
- Simultaneous Analysis of Common Oxyhalides and Anions (SI-37 4D)
- Analysis of Oxyhalides in Artificial-Drinking Water According to EPA Method 300.1 (SI-37 4D)