ε-caprolactam, a residual monomer in nylon 6, was analyzed using Asahipak ODP-50 4D, a reversed-phase chromatography column. Analysis of ε-caprolactam can be performed without an influence from extract contaminants.
- Add 10 mL of pure water to 0.5 g of nylon 6 pellets. Seal and heat at 100 ℃ for 2 hours.
- Once the mixture is cooled to room temperature, filter through a 0.5μm filter. Use the filtrate as a test sample.
Sample: 10 μL
- 1.ε-Caprolactam
- Column
- :Shodex Asahipak ODP-50 4D (4.6 mm I.D x 150 mm)
- Eluent
- :H2O/CH3CN=80/20
- Flow rate
- :0.7 mL/min
- Detector
- :UV (210 nm)
- Column temp.
- :40 ℃
Sample Name Index
Operation Manual / Certificate of Analysis
Operation Manuals and Certificate of Analysis / Inspection Certificate for the following products can be downloaded here.
Product Name Index
Applications
- Phthalates and Alkylbenzenes (1) (KF-801)
- Phthalates and Alkylbenzenes (2) (KF-401HQ)
- Effects of Flow Rate on Plate Number (KF-802)
- Recycle Analysis of Impurity in Resin (H-2001)
- Analysis of Antioxidant in Polystyrene (GPC/MS) (KF-402HQ)
- Analysis of IRGANOX® 1010 in Cup of Instant Noodles (Styrene Foam) (GPC/MS) (KF-402HQ)
- Simultaneous Analysis of Various Additives of Polymer in Polystyrene (GPC/MS) (KF-402HQ)
- Analysis of High Molecular Weight Hindered Amine Light Stabilizers (HALS) (GF-310 HQ)