li l46570598843567059210521354672135467569813753412012345054123656751423756419870505052468246812123426min239898 IonExcusonChromatography CoumnsColumn Eluent Flow rate Detector Column temp. : 75 ˚C: Shodex SUGAR SH1821 : 0.5 mM H2SO4 aq. : 0.6 mL/min : RI (1) Shodex SUGAR SH1011 8C(8.0 mm I.D. x 100 mm)(2) Ion exclusion column from other manufacturer (7.8 mm I.D. x 100 mm): (1) Shodex SUGAR SH1011 8C (2) Ion exclusion column from Column Eluent Flow rate Detector Column temp. : 65 ˚Cother manufacturer : 1 mM H2SO4 aq. : (1) 1.0 mL/min (2) 0.95 mL/min: RI Fine rice wineColumn Eluent Flow rate Detector : Shodex RSpak KC-G 8B + KC-811 x 2: 4.8 mM HClO4 aq.: 1.0 mL/min: VIS (430 nm)post column methodColumn temp. : 63 °CSample : 0.05 % each, 20 µL1. Maltotetraose2. Maltotriose3. Maltose4. Glucose5. Lactic acid6. Glycerin7. Acetic acid8. Methanol9. Ethanol1015Sample : 0.1 % each, 5 µL1. Maltotriose 4. Lactic acid 2. Maltose 5. Acetic acid6. Glycerin3. Glucose Sample : 100 µL1. Phosphoric acid etc.2. Citric acid3. Pyruvic acid4. Malic acid5. Succinic acid6. Lactic acid7. Fumaric acid8. Acetic acid9. Pyroglutamic acid1015202025minSample : 1. Citric acid 2. Tartaric acid 3. Pyruvic acid 4. Malic acid 5. Succinic acid 6. Glycolic acid 7. Lactic acid 8. Fumaric acid 9. Acetic acid10. Levulinic acid11. Pyroglutamic acid12. Propionic acid13. Isobutyric acid14. n-Butyric acid7. EthanolTP: 6,300TP: 2,90025min101520Column Eluent Flow rate Detector Column temp. : 60 ˚C Column Eluent Flow rate Detector Column temp. : 50 ˚CFermented liquor: Shodex SUGAR SH1821 : 2 mM H2SO4 aq. : 0.6 mL/min : RI : Shodex RSpak KC-811 x 2: 6 mM HClO4 aq.: 1.0 mL/min: VIS (430 nm)post column methodPure rice wineSample : 0.1 % each, 10 µL1. Cellopentaose 2. Cellotetraose3. Cellotriose4. Cellobiose5. Glucose6. Glyceric acid7. Acetic acid8. 5-HMF9. Furfural101520253035121011102025min1015204045min131430minCN-10 min25minHOCH2CH(OH)CH2OHHOCH2CH(OH)COOHColumn Eluent Flow rate Detector Column temp. : 60 ˚C: Shodex SUGAR SH1011 : 2 mM H2SO4 aq. : 0.6 mL/min : RI Column Eluent Flow rate Detector Column temp. : 40 ˚C: Shodex RSpak KC-811: 3 mM HClO4 aq.: 1.0 mL/min: RI: Shodex RSpak KC-811 6E: 1 mM H2SO4 aq.: Chloramine T solution: 4-Pyridinecarboxylic acid-Pyrazolone solution: (Eluent) 1.0 mL/min (Reagent) 0.5 mL/min each: VIS (638 nm)Column Eluent Reagent A Reagent B Flow rate Detector Column temp. : 40 ˚CReaction temp. : (Reagent A) 40 ˚C (Reagent B) 80 ˚CSample : 0.1 % each, 10 µL1. Glyceric acid2. Glycerin101520min3. Glucuronolactone 0.01 %5. Ethanol 0.05 %1015minSample : 10 µg/L each, 100 µLCNCl10 minMaltooligosaccharides, organic acids and ethanolRapid analysis of maltooligosaccharides,organic acids and ethanolCello-oligosaccharides and furfuralsOrganic acids in sakeCommon organic acidsAnalysis of cyanide ion and cyanogen chloride with post column methodGlycerin and glyceric acidGlucronolactone and organic acids31
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