H2OH2Oil —α-D-Talose LgandExchange Chromatography CoumnsH2OPharmacopoeia Method Relevant Columns• Standard columnsElution volumes of saccharides analyzed by Shodex columns[Partial list only; refer to our website for complete list]EP SC1011-7FSUGAR SC-G 6B (guard column)USPpak MN-4317.8 x 3006.0 x 504.0 x 250Product CodeF6379300F6700090F6379230See page 72 for USP-NF Column List. SubstancesArabinoseD-ArabitolDulcitolmeso-ErythritolD(-)-FructoseD(+)-FucoseD(+)-GalactoseGentiobioseGlucosemyo-InositolIsomaltoseIsomaltotriose1-KestoseKojibioseLactitolLactoseLactuloseMaltitolMaltoseMaltotrioseMannitolD-MannoseMelibioseNystosePalatinitPalatinosePanoseD(+)-RaffinoseRhamnoseD(-)-RiboseD(-)-SorbitolSorboseStachyoseSucroseTrehaloseTrehaluloseXylitolXylobioseD(+)-XyloseD-XyluloseColumn Eluent Flow ｒate Detector Column temp. : 80 ˚C: SUGAR SP0810, SC1011, KS-801: H2O: 1.0 mL/min: RIProduct NameSP0810SC101110.42 8.9115.8611.3320.1812.7612.7010.0911.05 8.8510.48 8.84 9.74 7.98 7.22 6.08 8.63 7.3012.77 8.86 7.68 6.26 7.09 5.75 6.79 5.75 7.56 6.2113.27 8.09 8.05 6.51 9.13 6.9912.23 8.26 7.85 6.34 7.48 5.8915.8011.1010.72 8.17 8.16 6.45 6.38 5.452 peaks2 peaks 7.84 6.45 7.14 5.78 7.14 5.78 9.77 8.2319.3513.6621.6113.31 9.67 8.03 6.82 5.57 7.54 6.2921.3312.59 7.62 6.27 8.92 6.9519.8713.14 8.16 6.68 9.21 7.9010.64 9.02Column Eluent Flow ｒate Detector Column temp. : 70 ˚C: SUGAR SC1211: H2O/CH3CN = 65/35: 1.0 mL/min: RIFunctional Group(Counter Ion)Sulfo (Ca2+)Sulfo (Ca2+)Sulfo (Ca2+)Elution volume (mL)KS-801 8.21 7.63 7.40 7.86 7.71 8.09 7.58 5.75 7.17 7.99 5.95 5.34 5.26 5.88 6.13 5.99 6.19 6.03 5.94 5.38 7.23 7.64 5.98 4.93 5.90 5.89 5.32 5.29 7.37 9.04 7.42 7.38 4.97 5.87 8.76 5.78 6.10 7.94 6.40 7.71 8.04Column Eluent Flow ｒate Detector Column temp. : 60 ˚C: SUGAR SZ5532: H2O/CH3CN = 25/75: 1.0 mL/min: RIParticle SizeColumn Size (mm)(µm)I.D. x Length 810 8Base Material: Styrene divinylbenzene copolymerSZ5532NH2P-50 4E 5.11 6.18 7.27 6.29 9.46 7.45 5.73 5.43 5.37 6.75 4.50 5.43 6.46 8.1010.5016.36 5.87 8.6112.63 9.9610.5715.1821.1727.5513.0920.11 9.6514.8216.3511.8210.1213.27 9.1610.7213.0411.82 8.6714.2413.7924.96 8.75 7.39 5.83 7.8411.6914.7020.0531.902 peaks12.73 8.0812.1216.8725.6016.3620.25 3.93 5.52 4.82 5.45 9.79 7.09 5.12 7.3536.22 7.9111.87 5.69 6.4710.8513.25 9.5411.68 7.77 6.10 5.65 9.05 4.55 6.58 4.06 5.41(—) Not detected (Column Eluent Flow ｒate Detector Column temp. : 30 ˚CShipping SolventSC1211 5.56 8.1611.28 6.27 5.90 4.96 4.98 4.76 7.87 6.67 4.07 4.65 6.77 9.03 5.01 4.232 peaks 3.99 4.43 8.6411.88 4.92 8.51 4.7810.16 4.48 5.07) Overlap with solvent peak: Asahipak NH2P-50 4E: H2O/CH3CN = 25/75: 1.0 mL/min: RI27
元のページ ../index.html#29